Protocol for preconcentration and quantification of microcystins using LC-MS
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United States Patent and Trademark Office
Abstract
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Methods for detecting and quantifying one or more microcystin compounds in a sample are described. The methods may include a preconcentration step, and generally utilize an LC-MS or LC-MS/MS analysis with an Orbitrap Fusion mass spectrometer. The methods provide excellent recoveries and limits of quantification of microcystins.
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Keywords
G01N33/68, G01N1/40, G01N30/02, G01N30/72, G01N30/86